Short Course Listings
 
Short Course

Course Information
Course Title: Chemistry Laboratory Techniques for the Chemist and Technician – A Comprehensive Review
Categories: 1 - Liquid Chromatography
2 - Atomic Spectrometry-Spectroscopy
3 - Gas Chromatography-Mass Spectrometry
4 - Infrared Spectroscopy
5 - Laboratory Information and Management
6 - X-Ray Spectrometry
Instructor(s): Bryan Ham, Aihui MaHam Course Number: 21
Affiliation: Department of Homeland Security
Course Date: 03/04/2017 - Saturday Course Length: 2 Day Course
Start Time: 08:30 AM End Time: 05:00 PM
Course Date 2: 03/05/2017 - Sunday    
Start Time: 08:30 AM End Time: 05:00 PM
Fee: $1100 ($1500 after 2/18/17) Textbook Fee: $150

Course Description
The objective of the course is to present a survey of analytical chemistry and instrumental analyses. The class begins with an introduction/refresher/review of the laboratory including safety, glassware, basic math, data treatment (statistics), graphing and Excel, lab solutions, acid base theory and titrations. A section is also devoted to the introduction and use of an example of a typical laboratory LIMS program. The course then quickly moves to the theory and application of analytical techniques such as spectroscopy including UV/Vis, fluorescence, FTIR, NMR, and metals analyses including AAS, AMS, XRF and XRD, and then chromatography including HPLC, SPE, TLC, GLC, GC-MS, SCX and CE. The course then completes with a short survey of modern mass spectrometry. The course includes the use of two working programs, the first an example of a typical laboratory LIMS used for sample logging and data input, and the second is a chemist and technicians toolkit used for numerous applications in the lab, for teaching, and for review.

Target Audience
There are 350,000 applied chemical technology professionals in the US workforce (ACS). Course targets chemists, lab techs, analysts, undergrad students. Lab managers and supervisors to observe the course, the course’s book, and the LIMS and ToolKit programs. Teachers and professors to use LIMS, Toolkit program, textbook to teach a lab and anal chem course.

Course Outline
The course is an introductory and refresher/review course to the chemistry laboratory including a survey of analytical chemistry and instrumental analyses in conjunction with a computer based toolkit program called ChemTech-ToolKit, and a Laboratory Information Management System LIMS program. The class begins with an introduction/refresher/review of the laboratory including safety, glassware, basic math, data treatment (statistics), graphing and Excel, lab solutions, acid base theory and titrations. A section is also devoted to the introduction and use of an example of a typical laboratory LIMS program. The course then quickly moves to the theory and application of analytical techniques such as spectroscopy including UV/Vis, fluorescence, FTIR, NMR, and metals analyses including AAS, AMS, XRF and XRD, and then chromatography including HPLC, SPE, TLC, GLC, and GC-MS.

The ChemTech program serves as a reference for chemists and technicians and as a teaching guide for lab technicians. The toolkit is accompanied by an analytical chemistry text book. The program features fully functional tutorials that involve user interaction featuring basic math and lab statistics including graphing, making lab solutions and buffers, titrations, and acid-base theory. Instrumental analyses include UV/Vis, Fluorescence, FTIR, NMR, atomic spectroscopy, gas chromatography, liquid chromatography, and mass spectrometry. The use of a LIMS program is also covered including logging in samples, inputting lab test results, searching samples, approving samples, and printing reports and CofA.

Introduction to the Analytical Laboratory
Chemist and Technician in the Analytical Laboratory
Laboratory Safety
Basic Mathematics in the Laboratory
Analytical Data Treatment (Statistics)
Plotting and Graphing in the Laboratory
Introduction to Microsoft Excel
Laboratory Solutions
Making Laboratory Solutions
Normality
Molarity
Acid Base Theory and Buffer Solutions
Titration as an Analytical Technique
Electrochemistry Introduction
Laboratory Information Management System (LIMS)
Intro to a working LIMS
Logging in samples
Data recording
Sample searching
Approving, archiving, and reporting samples
Spectroscopy
Ultraviolet/Visible (UV/Vis) Absorption Spectroscopy
Fluorescence Optical Emission Spectroscopy
Fourier Transform Infrared Spectroscopy (FTIR)
Nuclear Magnetic Resonance Spectroscopy (NMR)
Atomic Absorption Spectroscopy (AAS)
Atomic Emission Spectroscopy (AES)
Atomic Mass Spectrometry
X-ray Fluorescence (XRF) and X-ray Diffraction (XRD)
Chromatography - Introduction and Theory
High Performance Liquid Chromatography (HPLC)
Solid Phase Extraction (SPE)
Thin Layer Chromatography (TLC)
Gas Liquid Chromatography (GLC)
Gas Chromatography-Mass Spectrometry (GC-MS)

The class also includes a companion teaching, reference, and toolkit program called ChemTech-ToolKit.

Course Instructor's Biography
Dr. Bryan Ham has worked in analytical chemistry laboratories for over 20 years including petrochemical, environmental, foodstuff, and life sciences research, and has a doctorate in analytical chemistry. He has published 16 research papers in peer reviewed journals, encyclopedia chapters, and three books: Even Electron Mass Spectrometry with Biomolecule Applications, John Wiley & Sons, Inc., 2008; Proteomics of Biological Systems: Protein Phosphorylation Using Mass Spectrometry Techniques, John Wiley & Sons, Inc., 2012; Analytical Chemistry: A Chemist and Laboratory Technician’s Toolkit, John Wiley & Sons, Inc., 2015. He is currently working for the Department of Homeland Security at the U.S. Customs and Border Protection New York Laboratory. He is a member of the American Society of Mass Spectrometry (ASMS) and the American Chemical Society (ACS). His interests include the fundamentals of analytical chemistry and instrumental analyses as applied to modern analytical laboratories. Dr. Aihui MaHam is an expert in the field of inorganic materials chemistry, and their characterization utilizing instrumental analyses including SEM, XRD, XRF, ICP-OES, ARL-OES, and ICP-MS. She also specializes in nano-materials including the synthesis and characterization of chemical and biological nano-sensors. She has published numerous research papers including a recent review in the journal Small entitled Protein-Based Nanomaterial Platforms for Drug Delivery which has been cited over 240 times by other researchers. She is currently working for the Department of Homeland Security at the U.S. Customs and Border Protection New York Laboratory. Her current interests include the application of instrumental analyses as applied to the modern analytical laboratory.